Synthesizing and Studying the Structure of Ni(II) Complexes Containing 2-alkyliminomethyl Pyrene Ligands

Luong Xuan Dien, Nguyen Xuan Truong, Ngo Duc Quan, Ken-ichi Yamashita, Kenichi Sugiura

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Published Dec 23, 2018
DOI: https://doi.org/10.25073/2588-1140/vnunst.4809

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XUAN DIEN, Luong et al. Synthesizing and Studying the Structure of Ni(II) Complexes Containing 2-alkyliminomethyl Pyrene Ligands. VNU Journal of Science: Natural Sciences and Technology, [S.l.], v. 34, n. 4, dec. 2018. ISSN 2588-1140. Available at: <https://js.vnu.edu.vn/NST/article/view/4809>. Date accessed: 27 apr. 2024. doi: https://doi.org/10.25073/2588-1140/vnunst.4809.
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Vol 34 No 4
Section
Review Articles

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Abstract

Abstract: The 1(Ni) and Ni(II) complex was synthesized based on the reaction between
N,O-bidentate ligand 2-((methylimino)methyl) pyrene-1-ol (1) and nickel acetate in a mixed solvent of toluene, ethanol and NaOAc. The characters of the complex, such as elemental analysis (EA), IR, NMR, MS spectroscopy and single crystal X-ray diffraction, were investigated. With respect to the nickel atom, 1(Ni) complex adopts a distorted square planar trans-coordination geometry. Concerning the ligand arrangement, 1(Ni) complex has a step configuration with an angle of 35.5o between the mean planes of the pyrene rings in the two independent molecules and step distance S = 1.93 Å, whereas the referent nickel(II) bis(salicylaldiminato) takes a much smaller step configuration with an angle of 17.6o and step distance S = 0.845 Å (Chart 1). 


Keywords: Coordination chemistry, Nickel, Pyrene, expanded ligand, salicylaldimine.


References
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Keywords: Coordination chemistry, Nickel, Pyrene, π-Expanded ligand, Salicylaldimine

References

References
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[3] V. C. Gibson, S. K. Spitzmesser, Chem. Rev. 103 (2003) 283.
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[5] D. A. Bansleben, S. K. Freiedrich, T. R. Younkin, R. H. Grubbs, C. Wnag, R.T. Li (1998) WO98/03165.
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[9] W. H. Sun, H. Yang, Z. Li, Y. Li, Organometallics 22 (2003) 3678.
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[11] C. Carlini, M. Martinelli, A. M. R. Galletti, G. Sbrana, J. Polym. Sci. A 44 (2006) 1514.
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[13] M. Delferro, J. P. McInnis, T. J. Marks, Organometallics 29 (2010) 5040.
[14] D. J. Darensbourg, C. G. Ortiz, J. C. Yarbrough, Inorg. Chem. 42 (2003) 6915.
[15] H. Liang, J. Liu, X. Li, Y. Li, Polyhedron, 23 (2004) 1619.
[16] Y. Chen, S. Mandal, A. Sen, Organometallics 29 (2010) 3160.
[17] M. Kang, A. Sen, Organometallics 24 (2005) 3508.
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[23] Y. Murata, H. Ohgi, T. Fujihara, J. Terao, Y. Tsuji, Inorg. Chim. Acta 368 (2011) 237.
[24] T. Wiedemann, G. Voit, A. Tchernook, P. Roesle, I. Goettker-Schnetmann, S. Mecking, J. Am. Chem. Soc. 136 (2014) 2078.
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[35] L. Sacconi, M. Ciampolini, J. Chem. Soc. (1964) 276.
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